56 could signify the development of the dihydroazetium ion. All through GC Evaluation, a second products at 7.26 min was also observed within the chromatogram (Supporting Details) and it had been believed that this products might need been a degradant resulting in the thermal decomposition of 4F-MPH within the GC method.
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The nitrile intermediate was hydrolysed under acidic conditions bringing about the development of the acetamide species. Hydrogenation of the pyridine ring to piperidine followed, leading to the formation of two racemic erythro
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The instructed pathways are shown in Figure three. From the mass spectra of both racemates, the fragment noticed at m/z
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